| 1-环己烯乙腈制备1-环己烯乙胺的研究 |
| |
| 引用本文： | 宋长生,武宝萍,吴庆利,焦广俊,李树安.1-环己烯乙腈制备1-环己烯乙胺的研究[J].应用化工,2005,34(8):484-486. |
| |
| 作者姓名： | 宋长生 武宝萍 吴庆利 焦广俊 李树安 |
| |
| 作者单位： | 淮海工学院,化工系,江苏,连云港,222005 |
| |
| 摘 要： | 采用间接合成法,以1-环己烯乙腈为原料合成1-环己烯乙胺。重点考察了反应温度、反应压力、反应时间对产物1-环己烯乙胺收率的影响,得出最佳反应条件为:反应温度150℃、反应压力1.2 MPa、反应时间1.5 h,在此条件下,得到1-环己烯乙胺的最佳收率为85.3%。
|
| 关 键 词： | 1-环己烯乙胺 正交设计 合成 |
| 文章编号： | 1671-3206(2005)08-0484-03 |
| 修稿时间： | 2005年6月8日 |
Synthesis of 1-cyclohex-1-en-1-ethylamine from cyclohex-1-en-1-acetonitrile |
| |
| SONG Chang-sheng,WU Bao-ping,WU Qing-li,JIAO Guang-jun,LI Shuan.Synthesis of 1-cyclohex-1-en-1-ethylamine from cyclohex-1-en-1-acetonitrile[J].Applied chemical industry,2005,34(8):484-486. |
| |
| Authors: | SONG Chang-sheng WU Bao-ping WU Qing-li JIAO Guang-jun LI Shuan |
| |
| Abstract: | 1-Cyclohex-1-en-1-ethylamine was synthesized from cyclohex-1-en-1-acetonitrile by indirect synthetic method.The effect of reaction temperature,reaction pressure and reaction time on the synthesis of 1-cyclohex-1-en-1-ethylamine were emphatically studied.The optimal reaction conditions have been obtained: reaction temperature is 150℃,reaction pressure is 1.2 MPa,reaction time is 1.5 h,under this condition,the yield of 1-cyclohex-1-en-1-ethylamine is up to 85.3% at last. |
| |
| Keywords: | 1-cyclohex-1-en-1-ethylamine orthogonal design test synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
