| 两步浸蚀法预处理对火焰法沉积金刚石膜形貌、结构和性能的影响 |
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| 引用本文： | 朱晖朝,雷淑梅,陈丽凤,朱红梅,朱斌,匡同春.两步浸蚀法预处理对火焰法沉积金刚石膜形貌、结构和性能的影响[J].硬质合金,2009,26(3):148-151. |
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| 作者姓名： | 朱晖朝 雷淑梅 陈丽凤 朱红梅 朱斌 匡同春 |
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| 作者单位： | 1. 广州有色金属研究院,广东,广州,510651
2. 华南理工大学分析测试中心,广东广州,510641 |
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| 基金项目： | 广东省科技计划项目(工业攻关计划) |
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| 摘 要： | 两步浸蚀法是有效改善硬质合金基体表面沉积金刚石膜质量的一种预处理方法。本文采用两种不同酸剂的两步浸蚀法分别对YG6硬质合金基体进行了表面预处理,然后在其上火焰法沉积金刚石膜,初步探讨了预处理工艺不同酸剂对金刚石膜形貌、组成和结构的影响。实验结果表明,两步浸蚀法预处理能有效抑制合金基体中粘结相Co促进石墨生长的催化效应,两种火焰沉积产物已连续成膜,主要为超细金刚石、少量石墨。
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| 关 键 词： | 两步浸蚀法 扩散火焰 硬质合金 金刚石膜 |
Effect of Two-step Etching Pretreatment on Diamond Films Flame-deposited onto Hardmetal |
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| Zhu Huichao,Lei Shumei,Chen Lifeng,Zhu Hongmei,Zhu Bin,Kuang Tongchun.Effect of Two-step Etching Pretreatment on Diamond Films Flame-deposited onto Hardmetal[J].Cemented Carbide,2009,26(3):148-151. |
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| Authors: | Zhu Huichao Lei Shumei Chen Lifeng Zhu Hongmei Zhu Bin Kuang Tongchun |
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| Affiliation: | Zhu Huichao, Lei Shumei,Chen Lifeng, Zhu Hongmei, Zhu Bin,Kuang Tongchun(1.Guangzhou Research Institute of Non-ferrous Metals, Guangzhou Guangdong 510651, 2. Analytical and Testing Center, South China University of Technology, Guangzhou Guangdong 510641) |
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| Abstract: | Two-step etching pretreatment is proved to effectively improve the quality of diamond film deposited onto hardmetal substrate. Different two-step methods using various acids have been utilized for the cobalt cemented tungsten carbide （WC-6%Co, hereafter referred to as simply YG6）, then diamond films were deposited onto them by diffusion game. The effect of different pretreatment process on the morphology, compositions and microstructure of the diamond film are preliminarily discussed. The results showed that two-step pretreatment method can restrain the cobalt catalytic effect of graphitization. The two kinds of flame-deposited materials form continuous film. They are mainly ultrafine diamond and fewer graphite. |
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| Keywords: | two-step method diffusion flame hardmetal diamond film |
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