| 合成1,2-二氟代碳酸乙烯酯的研究 |
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| 引用本文： | 张洪源,王瑞,叶学海,刘红光.合成1,2-二氟代碳酸乙烯酯的研究[J].山东化工,2014(6):10-11. |
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| 作者姓名： | 张洪源 王瑞 叶学海 刘红光 |
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| 作者单位： | 中海油天津化工研究设计院新材料重点实验室,天津300131 |
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| 摘 要： | 以氟气为加成试剂,在以二氯甲烷为溶剂的体系中与碳酸亚乙烯酯发生加成反应生成1,2-二氟代碳酸乙烯酯,重点讨论了氟气的流量对反应速率的影响,根据反应性质开发了新式反应器,并对比了新式反应器与传统反应器对反应速率的影响。
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| 关 键 词： | 氟气 合成 加成反应 1 2-二氟代碳酸乙烯酯 |
The Research on Synthesis of Di -fluoro Ethylene Carbonate |
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| ZHANG Hongyuan,WANG Rui,YE Xuehai,LIU Hongguang.The Research on Synthesis of Di -fluoro Ethylene Carbonate[J].Shandong Chemical Industry,2014(6):10-11. |
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| Authors: | ZHANG Hongyuan WANG Rui YE Xuehai LIU Hongguang |
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| Affiliation: | (CNOOC Tianjin Chemical Research and Design Institute, Tianjin 300131 ,China) |
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| Abstract: | Fluorine and vinylene carbonate were employed to attend the addition reaction. The Di -fluoro ethylene carbonate was gained at the solvent dichloromethane. The gas flow was discussed, and then the new reactor was designed according the reaction character. |
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| Keywords: | fluorine synthesis addition reaction dDi- fluoro ethylene carbonate |
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