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离子束辅助沉积合成B—N薄膜的分析
引用本文:江海,陶琨,李恒德.离子束辅助沉积合成B—N薄膜的分析[J].金属学报,1993,29(4):77-80.
作者姓名:江海  陶琨  李恒德
作者单位:清华大学材料科学与工程系,清华大学,清华大学 讲师,北京 100084
摘    要:用离子束辅助沉积(IBAD)技术合成氮化硼薄膜,红外吸收谱和透射电镜的观测结果显示,薄膜含有c—BN和h—BN相薄膜Knoop硬度值高达35GPa。逐层剥离的AES谱结果表明,薄膜表面存在氮离子的注入效应,薄膜由注入层、成分均匀层和离子束混合过渡层组成

关 键 词:氮化硼  薄膜  IBAD
收稿时间:1993-04-18
修稿时间:1993-04-18

PREPARATION OF B-N FILMS BY ION BEAM ASSISTED DEPOSITION
JIANG Hai,TAO Kun,LI Hengde Tsinghua University.PREPARATION OF B-N FILMS BY ION BEAM ASSISTED DEPOSITION[J].Acta Metallurgica Sinica,1993,29(4):77-80.
Authors:JIANG Hai  TAO Kun  LI Hengde Tsinghua University
Affiliation:JIANG Hai,TAO Kun,LI Hengde Tsinghua University. Beijing lecturer,Department of Materials Science and Engineering,Tsinghua University,Beijing
Abstract:BN films, synthesized by ion beam assisted deposition, were analysed by RBS,AES, IR spectra and TEM. Formation of c-BN phase was shown not only by IR spectra atabsorption peak of 1100 cm~(-1), but also by electron diffraction pattern. The results of AESdemonstrate an effect of N~+ implantation near the film surface. The deposited films consist ofthree layers, i.e., ion implantation layer, film layer and mixed intermediate layer, according tothe difference of concentration. The micro-Knoop hardess of the film is 25-35 GPa.
Keywords:ion beam assisted deposition  BN film
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