| 2,6-二(4-氯甲酰苯氧基)苯甲腈的合成与表征 |
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| 引用本文： | 余义开,蔡明中,叶尚辉,彭以元,桑晓燕,黄宜祥.2,6-二(4-氯甲酰苯氧基)苯甲腈的合成与表征[J].河南化工,2006,23(5):10-12. |
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| 作者姓名： | 余义开 蔡明中 叶尚辉 彭以元 桑晓燕 黄宜祥 |
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| 作者单位： | 江西师范大学,化学化工学院,江西,南昌,330022 |
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| 摘 要： | 在KOH及DMSO的存在下,先将对羟基苯甲酸(p-HDBC)与2,6-二氟苯甲腈(DFBN)进行缩合反应生成2,6-二(4-羧苯氧基)苯甲腈(BCPOBN),BCPOBN与氯化亚砜反应,得到2,6-二(4-氯甲酰苯氧基)苯甲腈(BClPOBN).
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| 关 键 词： | 对羟基苯甲酸 2 6-二氟苯甲腈 2 6-二(4-氯甲酰苯氧基)苯甲腈 |
| 文章编号： | 1003-3467（2006）05-0010-02 |
| 收稿时间： | 2006-02-06 |
| 修稿时间： | 2006-02-06 |
Synthesis and Characterization of 2, 6-Bis(4-chloroformylphenoxyl) Benzonitrile |
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| YU Yi-kai,CAI Ming-zhong,YE Shang-hui,PENG Yi-yuan,SANG Xiao-yan,HUANG Yi-xiang.Synthesis and Characterization of 2, 6-Bis(4-chloroformylphenoxyl) Benzonitrile[J].Henan Chemical Industry,2006,23(5):10-12. |
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| Authors: | YU Yi-kai CAI Ming-zhong YE Shang-hui PENG Yi-yuan SANG Xiao-yan HUANG Yi-xiang |
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| Affiliation: | College of Chemistry and Chemical Engineering , Jiangxi Normal University , Nanchang 330022 , China |
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| Abstract: | 2,6-Bis(4-carboxyphenoxy) benzonitrile(BCPOBN) is prepared by condensation of 2,6-difluorobenzonitrile(DFBN) and p-hydroxybenzoic acid(p-HDBC) in the presence of KOH and DMSO.And then reaction of 2,6-bis(4-carboxyphenoxy)benzonitrile(BCPOBN) with sulfuryl dichloride yielded 2,6-bis(4-chloroformylphenoxy) benzonitrile(BClPOBN). |
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| Keywords: | p-hydroxybenzoic acid 2 6-difluorobenzonitrile 2 6-bis(4-chloroformylphenoxy) benzonitrile |
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