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正交实验优选青皮挥发油提取工艺
引用本文:曹蕾,赵国虎,赵军,曹纬.正交实验优选青皮挥发油提取工艺[J].化学与生物工程,2007,24(4):58-60.
作者姓名:曹蕾  赵国虎  赵军  曹纬
作者单位:1. 甘肃农业大学生命科学技术学院,甘肃,兰州,730070;甘肃农业大学理学院,甘肃,兰州,730070
2. 甘肃农业大学理学院,甘肃,兰州,730070
3. 兰州石油机械研究所,甘肃,兰州,730050
摘    要:采用水蒸气蒸馏法提取了中药青皮中的挥发油.以挥发油提取量为考察指标,以粉碎度、浸泡时间、提取时间为考察因素进行正交实验,优选了最佳提取工艺.结果表明,提取时间对青皮挥发油的提取有极显著影响(P<0.01),粉碎度影响显著(P<0.05),浸泡时间无显著影响(P>0.05).最佳提取工艺条件为:药材粉碎过80目筛,浸泡2 h,提取7 h.优选得到的工艺稳定可行.

关 键 词:青皮  挥发油  正交实验  提取工艺
文章编号:1672-5425(2007)04-0058-03
修稿时间:2007-01-04

Optimization of Extraction Process for Volatile Oil from Pericarpium Citri Reticulatae Viride by Orthogonal Test
CAO Lei,ZHAO Guo-hu,ZHAO Jun,CAO Wei.Optimization of Extraction Process for Volatile Oil from Pericarpium Citri Reticulatae Viride by Orthogonal Test[J].Chemistry & Bioengineering,2007,24(4):58-60.
Authors:CAO Lei  ZHAO Guo-hu  ZHAO Jun  CAO Wei
Affiliation:1.College of Life Science and Technology, Gansu Agricultural University, Lanzhou 730070, China; 2.College of Science; 3.Lanzhou Petroleum Machinery Research Institute, Lanzhou 730050, China
Abstract:The optimum extraction process for volatile oil from Pericarpium citri reticulatae viride was investigated by the L_9(34) orthogonal test.The volatile oils were extracted by the method of steam distillation,with the yield of volatile oil as index and three factors were chosen including the degree of crush,the soak time and the extraction time.The results showed that the effect of the extraction time was highly significant(P<0.01),the degree of crush was significant(P<0.05) and the soak time was not significant(P>0.05).The optimum extraction conditions were obtained as follows:powder of 80 eyelets,soaking for 2 hours and extracting for 7 hours.The optimized process is stable and highly efficient.
Keywords:Pericarpium citri reticulatae viride  volatile oil  orthogonal test  extraction process
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