Synthesis of micro-and nanosized PbS with different morphologies by the hydrothermal process期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

Synthesis of micro-and nanosized PbS with different morphologies by the hydrothermal process

Authors:	Fatemeh Davar Maryam Mohammadikish Mohammad Reza Loghman-Estarki Majid Masteri-Farahani

Affiliation:	1. Department of Chemistry, Isfahan University of Technology, Isfahan, Iran;2. Faculty of Chemistry, Kharazmi University, Tehran, Iran;3. Young Researchers and Elite Club, Kashan Branch, Islamic Azad University, Kashan, Iran

Abstract:	PbS micro- and nanostructures with different morphologies and particle sizes were obtained via a simple hydrothermal reaction between lead oxalate, Pb(C₂O₄)₂, and thioglycolic acid (TGA) as Pb²⁺ and the sulfur source and the capping agent, respectively. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet–visible (UV–vis) spectroscopy and Fourier transform infrared (FT-IR) spectra. The effects of temperature, reaction time and the type of Pb²⁺ source on the morphology and particle sizes of products were investigated.

Keywords:	Nanomaterials Semiconductors Hydrothermal Optical spectroscopy PbS
本文献已被 ScienceDirect 等数据库收录！