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| 正交法优选锂云母中提取铯的最佳条件 | |
| 引用本文： | 汤洪波,周健,梅光泉. 正交法优选锂云母中提取铯的最佳条件[J]. 应用化工, 2011, 0(10) |
| 作者姓名： | 汤洪波 周健 梅光泉 |
| 作者单位： | 宜春学院江西省高等学校应用化学与化学生物学重点实验室江西省天然药物活性成分研究重点实验室; |
| 基金项目： | 江西省高校重点实验室科技计划项目资助(赣教技字09640号) |
| 摘 要： | 用硫酸从锂云母中提取铯,采用正交设计表安排实验,用火焰原子吸收光谱法检测铯,以Cs2O水溶性浸出物含量为指标,对硫酸的质量分数,反应时间,液固质量比进行考察。结果表明,最佳工艺条件为:硫酸的质量分数为40%,反应时间为8 h,液固比为3∶1。在最佳条件下,100 g锂云母可提取Cs2O约150 mg。 |
| 关 键 词： | 正交设计 锂云母 铯 提取 |
The optimum extraction condition of cesium from lepidolite using orthogonal experiment design |
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| TANG Hong-bo,ZHOU Jian,MEI Guang-quan. The optimum extraction condition of cesium from lepidolite using orthogonal experiment design[J]. Applied chemical industry, 2011, 0(10) | |
| Authors: | TANG Hong-bo ZHOU Jian MEI Guang-quan |
| Affiliation: | TANG Hong-bo,ZHOU Jian,MEI Guang-quan(Key Laboratory of Jiangxi University for Applied Chemistry and Chemical Biology,Key Laboratory of Research on Active Ingredients in Natural Medicine of Jiangxi Province,Yichun College,Yichun 336000,China) |
| Abstract: | The cesium was extracted from lepidolite using sulfuric acid.The experiment was arranged by orthogonal experiment,cesium was determined by flame atomic absorption spectrometry.Based on the content of Cs2O water-soluble,the effect of mass fraction of sulfuric acid,reaction time,mass ratio of liquid to solid were studied.Results showed the optimum conditions were as follows:mass fraction of sulfuric acid 40%,reaction time 8 h,mass ratio of liquid to solid 3 ∶ 1.Under the optimum conditions,150 mg cesium could be extracted from 100 g lepidolite. |
| Keywords: | orthogonal experiment design lepidolite cesium extraction |
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