| 气-质联用法快速定性17种农药有效成分 |
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| 引用本文： | 黄晓华,吴玉琴,肖鸣,徐永.气-质联用法快速定性17种农药有效成分[J].现代农药,2011,10(2):27-29. |
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| 作者姓名： | 黄晓华 吴玉琴 肖鸣 徐永 |
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| 作者单位： | 浙江省农药检定管理所,杭州,310020 |
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| 摘 要： | 建立了杀虫剂农药中17种可能添加的未经登记农药成分的筛选方法。可疑成分首先通过气相色谱法保留时间进行初筛定性,再经过气相色谱质谱联用仪进行质谱解析确证。同时分析了影响保留时间的主要因子及提高定性准确性的方法,通过选择合适的定性碎片降低相互干扰。为管理部门监管农药生产企业擅自添加未经登记成分提供技术支持。
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| 关 键 词： | 未经登记成分 定性 杀虫剂 |
Rapid Qualitative Analysis of 17 Active Ingredients in Pesticide Using GC-MS |
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| HUANG Xiao-hua,WU Yu-qin,XIAO Ming,XU Yong.Rapid Qualitative Analysis of 17 Active Ingredients in Pesticide Using GC-MS[J].Modern Agrochemicals,2011,10(2):27-29. |
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| Authors: | HUANG Xiao-hua WU Yu-qin XIAO Ming XU Yong |
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| Affiliation: | HUANG Xiao-hua,WU Yu-qin,XIAO Ming,XU Yong(Intitute for the Control of Agrochemicals in Zhejiang Province,Hangzhou 310020,China) |
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| Abstract: | The qualitative analysis of 17 active ingredients unregistered was established.The retention time in GC and GC-MS was obtained in the test.The main factor of influence on peak resolution and to decrease the effect through GC-MS SIM mode was discussed. |
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| Keywords: | active ingredient unregistered qualitative analysis insecticide |
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