| 纳米Fe粉的制备研究 |
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| 引用本文： | 宫泮伟,李在元,翟玉春.纳米Fe粉的制备研究[J].微纳电子技术,2006,43(7):333-337,341. |
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| 作者姓名： | 宫泮伟 李在元 翟玉春 |
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| 作者单位： | 东北大学材料与冶金学院，东北大学材料与冶金学院，东北大学材料与冶金学院 沈阳110004辽宁石油化工大学石油化工分院，辽宁抚顺113001，沈阳110004，沈阳110004 |
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| 摘 要： | 总结了纳米Fe粉的制备方法,重点介绍了一种新的制备方法——封闭循环氢还原法。该方法以FeSO·47H2O和NaOH为原料,采用沉淀方法制备粒径为30～70nm的Fe2O3粉末,其反应条件为:反应温度50℃,反应终点pH值大于12,陈化时间1h。用封闭循环氢还原法,在400℃下还原Fe2O3得到了Fe粉。其粒径在20～50nm之间,含量为99.16%。
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| 关 键 词： | 铁 纳米粉 封闭循环氢还原 |
| 文章编号： | 1671-4776（2006）07-0333-05 |
| 收稿时间： | 2005-11-17 |
| 修稿时间： | 2005-11-17 |
Study on the Preparation of Fe Nano-Powders |
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| GONG Pan-wei,LI Zai-yuan,ZHAI Yu-chun.Study on the Preparation of Fe Nano-Powders[J].Micronanoelectronic Technology,2006,43(7):333-337,341. |
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| Authors: | GONG Pan-wei LI Zai-yuan ZHAI Yu-chun |
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| Affiliation: | GONG Pan-wei1,2,LI Zai-yuan1,ZHAI Yu-chun1 |
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| Abstract: | The preparation methods of Fe nano-powders were summarized.A new method was introduced--Seal circulation hydrogen reduction.The precursor of Fe2O3 was prepared with NaOH and FeSO4·7H2O using the chemical precipitation.The Fe2O3 particle size was 30～70 nm.The reacting temperature was 50 ℃,pH value of reacting terminal was 12,ageing time was 1 h.The even Fe nano-powders was prepared by reducing Fe2O3 at 400 ℃.The Fe particle size was 20～50 nm,purity was 99.16%. |
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| Keywords: | Fe nano-powders seal circulation hydrogen reduction |
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