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活性炭富集、原子吸收分光光度法测定工业废料中的金
引用本文:李小玲. 活性炭富集、原子吸收分光光度法测定工业废料中的金[J]. 广东有色金属学报, 2004, 14(2): 151-153
作者姓名:李小玲
作者单位:广州有色金属研究院分析测试中心 广东
摘    要:
用活性炭富集、原子吸收分光光度法测定工业废料中的金.首先选取有代表性的试样.其次溶样时先用混合酸将样品中的有机物氧化完全,再加王水溶金;为使金富集完全分取适量试液用活性炭富集金,并用HCl和NH4HF2对吸附金的活性炭洗涤除杂.本法测定结果与火试金法测定结果一致,但本法分析成本低、毒性小、分析快速,相对标准偏差小于1.20%。

关 键 词:原子吸收分光光度法 试液 测定结果 毒性 HC 适量 分析 活性炭 并用 工业废料

Determination of gold in industrial waste by activated carbon concentration and atomic absorption spectrophotometry
LI Xiao-ling. Determination of gold in industrial waste by activated carbon concentration and atomic absorption spectrophotometry[J]. Journal of Guangdong Non-Ferrous Metals, 2004, 14(2): 151-153
Authors:LI Xiao-ling
Abstract:
Gold in industry waste is determined by activated carbon concentrationa and atomic absorption spec trophotometry. First, sample must be selected. Secondary, organism in the sample is oxidized with mixed acid, and gold in it is dissolved with aquaregia. A part of test solution is taken in order to concentrate gold completly with activated carbon. The activated carbon adsorpted gold is washed with HC1 and NH4HF2, and meantime some impurities in it are removed. The results of this method are in conformity with the those of fire assaying. But the method is characterized with a low analytical cost, little pollution, fast analysis and relative standard deviation less than 1.20 % .
Keywords:atomic absorption spectrophotometry  industrial waste  gold  
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