| 层状纳米羟基磷灰石的制备及影响因素 |
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| 引用本文： | 王迎军,刘小健,魏坤,张淑花,任力,赵娜如,赖琛.层状纳米羟基磷灰石的制备及影响因素[J].硅酸盐学报,2007,35(9):1200-1204. |
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| 作者姓名： | 王迎军 刘小健 魏坤 张淑花 任力 赵娜如 赖琛 |
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| 作者单位： | 1. 华南理工大学材料科学与工程学院,广州,510640;华南理工大学特种功能材料教育部重点实验室,广州,510640
2. 华南理工大学材料科学与工程学院,广州,510640 |
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| 基金项目： | 国家自然科学基金
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国家重点基础研究发展计划(973计划) |
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| 摘 要： | 以表面活性剂磷酸酯为模板剂制备了具有层状结构的纳米羟基磷灰石(nano-hydroxyapatite,n-HA),该层状结构呈规则的周期性排列,层间距约为3.5 nm.用透射电子显微镜、广角X射线衍射、小角X射线衍射和Fourier变换红外光谱对材料的相组成、微观结构和形貌进行分析和表征.研究了液相体系中表面活性剂的浓度及反应温度对n-HA结构和形貌的影响.结果表明:反应温度和表面活性剂的浓度会显著影响材料的结构,最佳合成条件下可以形成相对均一的层状长条形n-HA.
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| 关 键 词： | 纳米羟基磷灰石 层状结构 表面活性剂 nano-hydroxyapatite layered structure surfactant |
| 文章编号： | 0454-5648（2007）09-1200-05 |
| 修稿时间： | 2007-01-04 |
SYNTHESIS AND INFLUENCE FACTORS OF NANO HYDROXYAPATITE WITH LAYERED STRUCTURE |
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| WANG Yingjun,LIU Xiaojian,WEI Kun,ZHANG Shuhua,REN Li,ZHAO Naru,LAI Chen.SYNTHESIS AND INFLUENCE FACTORS OF NANO HYDROXYAPATITE WITH LAYERED STRUCTURE[J].Journal of The Chinese Ceramic Society,2007,35(9):1200-1204. |
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| Authors: | WANG Yingjun LIU Xiaojian WEI Kun ZHANG Shuhua REN Li ZHAO Naru LAI Chen |
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| Affiliation: | 1. College of Materials Science and Engineering, South China University of Technology; 2. Key Laboratory of Specially Functional Materials, Ministry of Education, Guangzhou 510640, China |
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| Abstract: | Ordered multi-layered structure nano-hydroxyapatite (n-HA), with about 3.5 nm layer spacer, was synthesized using an organic phosphate as a template. The phase composition, microstructure and morphology of the n-HA were studied by transmission electron microscope , wide angle X-ray diffraction, small angle X-ray diffraction, and Fourier transform infrared spectroscopy. The effects of the surfactant concentration and reaction temperature on the microstructure of n-HA were investigated, and the morphology of the n-HA was also characterized. The results indicate that both the reaction temperature and the surfactant concentration greatly affected the microstructure and morphology of the n-HA. The optimized synthesis conditions of the uniform strip-like n-HA, with a layered structure, were obtained. |
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| Keywords: | nano-hydroxyapatite layered structure surfactant |
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