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| 1-氟-二苯[a,d]环庚酮的合成 | |
| 引用本文： | 李雯,闫学斌,朱成功. 1-氟-二苯[a,d]环庚酮的合成[J]. 化学试剂, 2006, 28(7): 443-443,445 |
| 作者姓名： | 李雯 闫学斌 朱成功 |
| 作者单位： | 郑州大学,化工学院,河南,郑州,450002;郑州大学,新药研究中心,河南,郑州,450052;河南辅仁集团,河南,郑州,450008 |
| 摘 要： | 以邻苯二甲酸酐和邻氟苯乙酸为原料,经高温缩合、还原、环化得到1-氟二苯[a,d]环庚酮,总收率为33.2%。该方法操作较简便,收率较高,具有工业生产价值。 |
| 关 键 词： | 1-氟-二苯[a d]环庚酮 缩合 还原 环化 合成 |
| 文章编号： | 0258-3283（2006）07-0443-01 |
| 收稿时间： | 2005-12-04 |
| 修稿时间： | 2005-12-04 |
The synthesis of 1-fluoro-dibenzo [ a, d] cycloheptanone |
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| LI Wen,YAN Xue-bin,ZHU Cheng-gong. The synthesis of 1-fluoro-dibenzo [ a, d] cycloheptanone[J]. Chemical Reagents, 2006, 28(7): 443-443,445 | |
| Authors: | LI Wen YAN Xue-bin ZHU Cheng-gong |
| Affiliation: | 1. College of Chemical Engineering, Zhengzhou University, Zhengzhou 450002, China; 2. Research Center of New Drug, Zhengzhou University, Zhengzhou 450052, China; 3. Henan Furen Group, Zhengzhou 450008, China |
| Abstract: | 1-Fluoro-dibenzo[a,d]cycloheptanone was synthesized from phthalic anhydride and orthofluorophenyl acetic acid as raw material by condensation under high temperature,reduction and cyclization.The total yield reached 33.2%.The method has high industrial value for its simplicity and high yield. |
| Keywords: | 1-fluoro-dibenzo[a d]cycloheptanone condensation reduction cyclization |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |