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微波法溶解废旧锌-锰电池正极活性物中锰的溶解条件的研究
引用本文:林曼斌,李春英. 微波法溶解废旧锌-锰电池正极活性物中锰的溶解条件的研究[J]. 广东化工, 2004, 31(7): 8-10
作者姓名:林曼斌  李春英
作者单位:韩山师范学院化学系,潮州,521041;韩山师范学院化学系,潮州,521041
摘    要:用盐酸-过氧化氢混合溶剂溶解废旧干电池正极活性物,用微波炉加热后,锰可定量留在溶液中,用高碘酸钾加热显色光度法测定锰的含量.适宜的溶解条件:盐酸浓度2mol/L,加热时间60s,过氧化氢浓度3%,微波炉火力20%,固液比0.2g:12ml.

关 键 词:废旧干电池  正极活性物  分光光度法  微波辐射法  
修稿时间:2004-04-01

Study on the Conditions of Dissolving Manganese in Anode Active Materials of Waste Zn-Mn Batteries by Microware Radiation
Lin Manbin Li Chunying. Study on the Conditions of Dissolving Manganese in Anode Active Materials of Waste Zn-Mn Batteries by Microware Radiation[J]. Guangdong Chemical Industry, 2004, 31(7): 8-10
Authors:Lin Manbin Li Chunying
Abstract:The determination method of manganese in anode active materials of waste Zn-Mn batteries using HCL-H2O2 fusion method heated by microware oven was briefly described manganese will be dissolved in solvent.Then suitable conditions were HCl-2mol/L; H2O2-3%; heated time-60s; microwares efficiency-20%; liquid:solid-0.2:12ml. The measuring the content of manganese whit 724-visible spectrophotometers.
Keywords:Waste Zn-Mn batteries  Microware radiation   Anode active materials  Manganese  Spectrophotometera
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