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响应曲面法漂白紫胶微波-真空干燥工艺研究
引用本文:于连松,张弘,郑华,周梅村,陈晓鸣,陈军,张雯雯.响应曲面法漂白紫胶微波-真空干燥工艺研究[J].陕西化工,2012(1):37-43.
作者姓名:于连松  张弘  郑华  周梅村  陈晓鸣  陈军  张雯雯
作者单位:[1]中国林业科学研究院资源昆虫研究所,国家林业局特色森林资源工程技术研究中心,云南昆明650224 [2]昆明理工大学化学工程学院,云南昆明650224
基金项目:科技部农业科技成果转化资金项目(2010GB24320619); 国家林业局“948”项目(2008-4-78); 国家林业科技成果推广项目([2010]11)
摘    要:为提高漂白紫胶产品质量及生产效率,采用微波-真空干燥漂白紫胶研究了不同压强、微波功率和干燥时间对漂白紫胶产品颜色指数和含水率的影响,用响应曲面法(RSM)设计试验并建立了该工艺条件的拟合方程。结果表明,拟合方程的拟合度较高,所建立的数学模型可以用于描述漂白紫胶的微波-真空干燥。漂白紫胶微波-真空干燥的最优条件:干燥压强为3.0 kPa,微波功率为795 W,干燥时间为30 min。在优化条件下进行了验证实验,得到了颜色指数为0.9、含水率为0.028 9kg水/kg干料的产品。

关 键 词:漂白紫胶  微波-真空干燥  响应曲面法

Research on microwave-vacuum drying process of bleached shellac by response surface method
YU Lian-song,ZHANG Hong,ZHENG Hua,ZHOU Mei-cun,CHEN Xiao-ming,CHEN Jun,ZHANG Wen-wen.Research on microwave-vacuum drying process of bleached shellac by response surface method[J].Applied Chemical Industry,2012(1):37-43.
Authors:YU Lian-song  ZHANG Hong  ZHENG Hua  ZHOU Mei-cun  CHEN Xiao-ming  CHEN Jun  ZHANG Wen-wen
Affiliation:1.Research Institute of Resource Insects,Chinese Academy of Forestry,Research Center of Engineering and Technology on Forest Resources with Characteristics,State Forestry Administration,Kunming 650224,China;2.Faculty of Chemical Engineering,Kunming University of Science and Technology,Kunming 650224,China)
Abstract:In order to improve product quality and production efficiency,effect of different pressure,microwave power and drying time on color index and moisture content of the products were studied by microwave-vacuum drying process of bleached shellac.Fitting equation of the process conditions was set up by response surface method(RSM) experimental design.Results showed that the equation was well fitting and the established mathematical model can be used to describe microwave-vacuum drying of bleached shellac.The optimal process may be taken at the pressure of 3 kPa with 795 W microwave power for 30 min drying.Under the optimal conditions,it can be achieved products with color index of 0.9 and moisture content of 0.028 9 kg water/kg dry materials.
Keywords:bleached shellac  microwave-vacuum drying  response surface method
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