| 扑炎痛合成工艺优化 |
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| 引用本文： | 马艳.扑炎痛合成工艺优化[J].化工时刊,2014(3):19-20. |
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| 作者姓名： | 马艳 |
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| 作者单位： | 山东中医药大学药学院,山东济南250355 |
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| 摘 要： | 取酯化反应中所用的溶剂、时间、相转移催化剂作为3因素,设计正交试验。得到了扑炎痛的最佳合成工艺。3个因素对扑炎痛收率的影响程度为:溶剂时间相转移催化剂。扑炎痛合成工艺的最佳组合方式:苯为溶剂,时间为1.5 h,相转移催化剂为溴化四丁基铵。
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| 关 键 词： | 扑炎痛 合成 三因素三水平 |
Improved Synthesis of Benorilate |
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| Ma Yan.Improved Synthesis of Benorilate[J].Chemical Industry Times,2014(3):19-20. |
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| Authors: | Ma Yan |
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| Affiliation: | Ma Yan ( College of Pharmacy, Shandong University of Traditional Chinese Medicine, Shandong Jinan 250355 ) |
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| Abstract: | The best synthesis of Benorilate was determined using. Orthogonal design. The influence of Benorilate yield level three factors were： solvent time phase transfer catalyst. The best combination on synthesis of inflammatory pain was benzene solvents,1. 5 hours,four tetrabutylammonium bromide as phase transfer catalyst. |
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| Keywords: | benorilate synthesize three factors and three levels |
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