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Optimisation of pectin acid extraction from passion fruit peel (Passiflora edulis flavicarpa) using response surface methodology
Authors:Erika Kliemann,Karina Nunes de Simas,Edna R. Amante,Elane Schwinden Prudê  ncio,Reinaldo F. Teó  filo,Má  rcia M. C.Ferreira,&   Renata D. M. C. Amboni
Affiliation: Department of Food Science and Technology, Center of Agricultural Science, Federal University of Santa Catarina, Rod. Admar Gonzaga, 1346, Itacorubi, 88034-00, Florianópolis, SC, Brazil;
 Institute of Chemistry, State University of Campinas, P.O.B. 6154, 13084-971 Campinas, SP, Brazil
Abstract:Pectin was extracted from passion fruit peel using three different acids (citric, hydrochloric or nitric) at different temperatures (40–90 °C), pH (1.2–2.6) and extraction times (10–90 min), with and without skins using a 24 factorial design. Temperature, pH and extraction time had highly significant effects on the pectin yield. A central composite design with face centring was used to optimise the extraction process conditions for citric acid without skins. Pectin yields varied from 10% to 70%. The optimal conditions for maximisation of pectin yield were the use of citric acid at 80 °C and pH 1 with an extraction time of 10 min considering model extrapolation.
Keywords:Central composite design    extraction yield    passion fruit    pectin    response surface methodology
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