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二羟基芦竹碱新型环保防污涂料的研制
引用本文:杨保平,邢杰,郭军红,谭生,李延华,崔锦峰.二羟基芦竹碱新型环保防污涂料的研制[J].现代涂料与涂装,2010,13(10):3-5.
作者姓名:杨保平  邢杰  郭军红  谭生  李延华  崔锦峰
作者单位:兰州理工大学石油化工学院,兰州,730050
摘    要:介绍了新型防污剂二羟基芦竹碱的应用与合成。以吲哚和二乙醇胺、甲醛为原料,在乙酸催化下合成了二羟基芦竹碱。通过正交试验给出最佳合成条件:反应时间6 h,反应温度25℃,pH为11。用FT-IR1,HNMR对合成的防污剂进行了表征。并将此防污剂应用到防污涂料中,进行杀菌试验,结果表明,此防污涂料具有明显的杀菌性能。

关 键 词:二羟基芦竹碱  曼尼希反应  防污涂料  生物毒性测试

The Development of 2-hydroxy Gramine New Antifouling and Environmental Coatings
Yang Baoping,Xing Jie,Guo Junhong,Tan Sheng,Li Yanhua,Cui Jinfeng.The Development of 2-hydroxy Gramine New Antifouling and Environmental Coatings[J].Modern Paint and Finishing,2010,13(10):3-5.
Authors:Yang Baoping  Xing Jie  Guo Junhong  Tan Sheng  Li Yanhua  Cui Jinfeng
Affiliation:Yang Baoping,Xing Jie,Guo Junhong,Tan Sheng,Li Yanhua,Cui Jinfeng
Abstract:The application and sythetic of 2-hydroxy gramine;a new antifouling agent.which is 2-hydroxy gramine was synthesized using indole,diethanolamine,and formaldehyde as initial reagents,and acetic acid as the catalyst.Optimum synthesis conditions were investigated by experiments utilizing an orthogonal design.Optimum 2-hydroxy gramine yields were obtained as follows: reaction time was 6 h;reaction temperature was 25 ℃;pH=11.The synthetic of 2-hydroxy gramine was characterized by rourier transform infrared ray(FT-IR) and 1HNMR.The new antifouling agent was applied to antifouling coatings.The bactericidal properties of antifouling coatings were analyzed by photosynthetic bacteria test.The effects of bactericidal properties were studied.
Keywords:2-hydroxy gramine  mannich reaction  anti-fouling coatings  biological toxicity test
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