| 气相色谱-质谱联用法检测保健品中8种安眠镇静类药物 |
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| 引用本文： | 王占良,张建丽,张亦农.气相色谱-质谱联用法检测保健品中8种安眠镇静类药物[J].质谱学报,2009,30(5):282-286. |
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| 作者姓名： | 王占良 张建丽 张亦农 |
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| 作者单位： | 国家体育总局反兴奋剂中心，北京 100029 |
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| 摘 要： | 采用气相色谱-质谱联用法同时检测保健品中的地西泮，咪达唑仑，硝基安定，唑吡坦，氯硝安定，艾司唑仑，阿普唑仑和佐匹克隆。用叔丁基甲醚提取，甲基睾酮作为内标，HP-1MS色谱柱(17 m ×0.2 mm×0.11 mm )分离，程序升温，质谱检测。该方法的检测限和回收率均满足保健品日常检测的要求，前处理简单、快速、可靠。
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| 关 键 词： | 保健品 气相色谱-质谱 安眠镇静 |
| 收稿时间： | 2009-08-31 |
Detection of Eight Sedative-Hypnotic Agents in Nutriment Products by GC/MS |
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| WANG Zhan-liang,ZHANG Jian-li,ZHANG Yi-nong.Detection of Eight Sedative-Hypnotic Agents in Nutriment Products by GC/MS[J].Journal of Chinese Mass Spectrometry Society,2009,30(5):282-286. |
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| Authors: | WANG Zhan-liang ZHANG Jian-li ZHANG Yi-nong |
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| Affiliation: | China Anti-Doping Agency, The State Sport General Administration, Beijing 100029, China |
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| Abstract: | Total of 4 PDE-5 inhibitors (tadalafil, sildenafil, homosildenafil, vardenafil) were simultaneously detected by gas chromatography-mass spectrometry coupling with electronic ionization. The sample was extracted with the ethyl acetate and completely separated by HP-1MS column (17m ×0.2 mm×0.11mm) in linear temperature program. The method is simple, rapid and reliable. It is suitable for screening PDE-5 inhibitors in routine analysis for nutriment products. |
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| Keywords: | nutriment gaschromatography-massspectrometry PDE-5inhibitor |
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