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预蒸馏—异烟酸—巴比妥酸光度法测定土壤中的总氰化物
引用本文:张金碧,蔡彩仁.预蒸馏—异烟酸—巴比妥酸光度法测定土壤中的总氰化物[J].广东化工,2010,37(12):123-124,138.
作者姓名:张金碧  蔡彩仁
作者单位:[1]华南师范大学化学与环境学院,广东广州510631 [2]广州市番禺区环境监测站,广东广州511483
摘    要:文章主要提出利用预蒸馏-异烟酸-巴比妥酸光度法对土壤中的总氰化物进行测定。蒸馏预处理过程改用硫酸代替磷酸使得预处理效果更好;采用更合适的分析方法—异烟酸-巴比妥酸光度法。

关 键 词:土壤  总氰化物  蒸馏  异烟酸-巴比妥酸

Determination of Total Cyanide in Soil by Pre-distillation-Isonicotinic Acid-Barbituric Acid Spectrophotometry
Zhang Jinbi,Cai Cairen.Determination of Total Cyanide in Soil by Pre-distillation-Isonicotinic Acid-Barbituric Acid Spectrophotometry[J].Guangdong Chemical Industry,2010,37(12):123-124,138.
Authors:Zhang Jinbi  Cai Cairen
Affiliation:1. College of Chemistry and Environment, South China Normal University, Guangzhou 510631 ; 2. Panyu Environmental Monitoring Station, Guangzhou 511483, China)
Abstract:The paper focuseed on determination of total cyanide in soil by pre-distillation-isonicotinic acid-barbituric acid spectrophotometry. The pre-distillation process made use sulfuric acid instead of phosphoric acid which makes the pre-processing better. Used a more appropriate method of isonicotinic acid-barbituric acid spectrophotometry.
Keywords:soil  total cyanide  distillation  isonicotinic acid - barbituric acid
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