The Formation and Melting of 3He Clusters in Phase-Separated Solid 3He-4He Mixtures

Melting pressure measurements have been made on the³He-rich phase formed by cooling a solid mixture of 0.6%³He in⁴He through phase separation, at pressures between 2.78 and 3.56 MPa. For comparison, simultaneous observations were made with the mixture confined in the pores of a silver sinter and in an open volume connected to the same fill-line. Samples in the sinter cell solidify at higher pressures than the open cell and equilibrate more quickly. Both cells exhibit hysteresis between melting and freezing temperatures, and the transitions are broader in the open-volume cell. Relative to pure³He, the melting pressure is elevated by as much as 60 kPa in the sinter cell and 20 kPa in the open cell. The size of the pressure change on melting indicates that a large fraction of the³He remains solid at pressures below the melting curve, and this effect is more pronounced in the sinter cell. Measurements are in progress to measure the magnetisation through the magnetic ordering transition.