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溶胶-凝胶法制备(Nd,Bi)_4Ti_3O_(12)铁电薄膜
引用本文:侯芳,臧涛成,李建康.溶胶-凝胶法制备(Nd,Bi)_4Ti_3O_(12)铁电薄膜[J].桂林工学院学报,2010,30(1):107-110.
作者姓名:侯芳  臧涛成  李建康
作者单位:苏州科技学院,数理学院,苏州,215009
基金项目:国家自然科学基金青年基金,江苏省自然科学基金,苏州科技学院科研基金 
摘    要:采用溶胶-凝胶法在Pt/Ti/SiO2/Si基片上制备了(Nd,Bi)4Ti3O12薄膜。将薄膜于空气中分别进行每1层、每2层、每3层500℃预退火10 min,最后于氮气氛中680℃退火30 min。结果表明:预退火工艺对薄膜的结构和铁电性能都有影响:每一层预退火处理的薄膜具有较大的剩余极化值和最小的矫顽场(2Pr=47.8μC/cm2,2Ec=254 kV/cm)。所有薄膜都呈现良好的抗疲劳特性。

关 键 词:Nd掺杂  溶胶-凝胶法  铁电薄膜  铁电性能

Preparation of Ferroelectric (Nd,Bi)4Ti3O12 Thin Films in Sol-Gel Process
HOU Fang,ZANG Tao-cheng,LI Jian-kang.Preparation of Ferroelectric (Nd,Bi)4Ti3O12 Thin Films in Sol-Gel Process[J].Journal of Guilin University of Technology,2010,30(1):107-110.
Authors:HOU Fang  ZANG Tao-cheng  LI Jian-kang
Affiliation:(School of Mathematics and Physics,Suzhou University of Science and Technology,Suzhou 215009,China)
Abstract:(Nd,Bi)4Ti3O12 thin films are deposited on Pt/Ti/SiO2/Si substrates in sol-gel process.The films are preannealed at 500 ℃ for 10 min every layer,every two layers and every three layers respectively,in the air,until all the films annealed at 500 ℃ for 30 min in nitrogen atmosphere.The results reveal that the structures and ferroelectric properties of(Nd,Bi)4Ti3O12 thin films sensitively depend on the preannealing treatment.The film,when preannealed every one layer in the air,has the larger remanent polarization value and the least coercive field(2Pr = 47.8 μC/cm2,2Ec= 254 kV/cm).All the films exhibit fatigue-free characteristics.
Keywords:Nd-doped  sol-gel processing  ferroelectric thin films  ferroelectric properties
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