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Fabrication, property characterization and toughening mechanism of HA-ZrO2(CaO)/316L fibre composite biomaterials
Authors:JianPeng Zou  ZeQiang He  ZhongCheng Zhou  BaiYun Huang  QiYuan Chen and JianMing Ruan
Affiliation:(1) State Key Laboratory for Powder Metallurgy, Central South University, Changsha, 410083, China;(2) Institute of Chemistry and Chemical Engineering, Jishou University, Jishou, 416000, China;(3) Institute of Chemistry and Chemical Engineering, Central South University, Changsha, 410083, China
Abstract:HA-ZrO2(CaO)/316L fibre composites were successfully fabricated with vacuum sintering method and their properties and toughening mechanism were studied. The results showed that HA-ZrO2(CaO)/316L fibre biocomposite having 20 vol% fibres had optimal comprehensive properties with bending strength, Young’s modulus, fracture toughness and relative density equal to 140.1 MPa, 117.8 GPa, 5.81 MPa·m1/2 and 87.1%, respectively. The research also addressed that different volume ratios of the composites led to different metallographic microstructures, and that metallographic morphologies change regularly with volume ratios of the composites. 316L fibres were distributed randomly and evenly in the composites and the integration circumstance of the two phases was very well since there were no obvious flaws or pores in the composites. Two toughening mechanisms including ZrO2 phase transformation toughening mechanism and fibre pulling-out toughening mechanism existed in the compsites with the latter being the main toughening mechanism. Supported by the National Natural Science Foundation of China (Grant No. 50604017) and the Postdoctoral Science Foundation of Central South University
Keywords:vacuum sintering  fabrication  property characterization  toughening mechanism  biomaterials
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