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Determination of acephate,methamidophos and monocrotophos in crude palm oil
Authors:Chee Beng Yeoh  Ainie Kuntom  Selvarajan Dorasamy  Mohd Rizal Omar  Muhd Yusof Mohd Nor  Mohd Razali Mohd Noh
Abstract:
A method for the determination of acephate, methamidophos and monocrotophos in oil matrices is described. Pesticide residues in crude palm oil were extracted with acetonitrile, and a clean‐up process was performed by cooling the entire extract below 10 °C, followed by a discolouring process using a Carbograph SPE cartridge. The extract was analysed using gas chromatography coupled with a pulsed flame photometry detector. The limit of detection for the method was calculated from regression data, and the recovery test results were in the range of 85–109%.
Keywords:Oil  pesticide residue  clean‐up  PFPD  SPE
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