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微量加碱法制备聚合氯化铝
引用本文:赵东风,孟伟,王永强.微量加碱法制备聚合氯化铝[J].工业用水与废水,2009,40(2).
作者姓名:赵东风  孟伟  王永强
作者单位:中国石油大学(华东)化学化工学院环境系,山东,青岛,266555
基金项目:中国石油天然气集团公司科学研究与技术开发项目 
摘    要:采用微量加碱法制备聚合氯化铝絮凝剂,使用Al-Ferron逐时络合比色法对制得的样品进行表征。探讨了制备方法、碱化度、制备温度、AlCl3和NaOH浓度对制备产品的影响。结果表明:当碱化度为2.5,反应温度为70℃左右,参与反应的AlCl3和NaOH溶液浓度均为2 mol/L时,可获得Al13的质量分数为85%左右的产品。

关 键 词:聚合氯化铝  微量加碱法  逐时络合比色法

Synthesis of polyaluminium chloride with microinjection of base method
ZHAO Dong-feng,MENG Wei,WANG Yong-qiang.Synthesis of polyaluminium chloride with microinjection of base method[J].Industrial Water & Wastewater,2009,40(2).
Authors:ZHAO Dong-feng  MENG Wei  WANG Yong-qiang
Abstract:The polyaluminium chloride was prepared by microinjection of base method,and the prepared sample was characterized by Al-Ferron complex timed colorimetric method,the effects of preparation method,alkalization degree,reaction temperature,concentration of AlCl3 and NaOH on the product were discussed.The results showed that: when the alkalization degree was 2.5,the reaction temperature was about 70 ℃,the concentra-tion of AlCl3 and NaOH were both 2 mol / L,the product with Al13 mass fraction about 85% could be obtained.
Keywords:polyaluminium chloride  microinjection of base method  complex timed colorimetric method  
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