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吴茱萸药材水蒸气蒸馏-醇提过大孔树脂柱联用工艺研究
引用本文:张军,卫罡,单珊,林吉.吴茱萸药材水蒸气蒸馏-醇提过大孔树脂柱联用工艺研究[J].食品与药品,2009,11(3).
作者姓名:张军  卫罡  单珊  林吉
作者单位:广州中医药大学新药开发研究中心,广东广州510405
基金项目:广东省科技计划项目(2007B031404005)
摘    要:目的研究吴茱萸药材水蒸气蒸馏-醇提过大孔树脂柱联用工艺的提取效果。方法以挥发油得率、吴茱萸碱和吴茱萸次碱保留率及药材中生物碱和水溶性成分的HPLC图谱为指标,考察水蒸气蒸馏-醇提过大孔树脂柱联用工艺对保留吴茱萸有效成分的影响。结果吴茱萸药材水蒸气蒸馏-醇提过大孔树脂柱联用工艺保留了药材挥发油、生物碱、水溶性成分,显著降低了出膏率。结论水蒸气蒸馏-醇提过大孔树脂柱联用工艺是吴茱萸药材提取纯化的适宜工艺。

关 键 词:吴茱萸  水蒸气蒸馏  醇提  大孔吸附树脂

Study on Extraction of Fructus evodiae by Wet Distillation-Alcohol Extract Combined with Macroporous Adsorptive Resin
ZHANG Jun,WEI Gang,SHAN Shan,LIN Ji.Study on Extraction of Fructus evodiae by Wet Distillation-Alcohol Extract Combined with Macroporous Adsorptive Resin[J].Food and Drug,2009,11(3).
Authors:ZHANG Jun  WEI Gang  SHAN Shan  LIN Ji
Affiliation:New Drug R&D Center;Guangzhou University of Chinese Medicine;Guangzhou 510405;China
Abstract:Objective To investigate the extraction efficiency of Fructus evodiae by wet distillation-alcohol extract combined with macroporous adsorptive resin.Methods With the extraction yield of volatile oils,contents of evodiamine and rutaecarpine metered by HPLC as indexes,the extraction efficiency of the above-mentioned combined extraction method was evaluated.Results The volatile oils,alkaloids and water-soluble components from Fructus evodiae were obtained effectively and the paste yield was reduced by wet dist...
Keywords:Fructus evodiae  wet distillation  alcohol extract  macroporous adsorptive resin  
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