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三明产柿叶总黄酮的微波提取研究
引用本文:陈淑燕,周文富.三明产柿叶总黄酮的微波提取研究[J].化学与生物工程,2011,28(11):57-61.
作者姓名:陈淑燕  周文富
作者单位:三明学院化学与生物工程系,福建三明,365004
摘    要:采用微波法提取柿叶中总黄酮,探讨了乙醇质量浓度、微波辐射功率、固液比和微波辐射时间等因素对柿叶总黄酮提取率的影响,并用UV和FTIR对提取产物进行了表征.通过单因素实验和正交实验确定最佳提取条件为:乙醇质量浓度65%,固液比1∶ 25(g:mL),微波辐射功率300 W,微波辐射时间15 min(间歇作用5次,每次3 ...

关 键 词:柿叶  总黄酮  微波提取  正交实验

Study on Microwave Extraction of Total Flavones from Sanming Persimmon Leaves
CHEN Shu-yan,ZHOU Wen-fu.Study on Microwave Extraction of Total Flavones from Sanming Persimmon Leaves[J].Chemistry & Bioengineering,2011,28(11):57-61.
Authors:CHEN Shu-yan  ZHOU Wen-fu
Affiliation:CHEN Shu-yan,ZHOU Wen-fu(Department of Chemistry and Biological Engineering,Sanming University,Sanming 365004,China)
Abstract:The total flavones was extracted from persimmon leaves by microwave extraction method.The effects of ethanol mass concentration,microwave irradiation power,solid-liquid ratio(g∶mL) and microwave irradiation time on the extraction rate of total flavones from persimmon leaves were studied.The optimal extraction conditions were obtained by single factor experiment and orthogonal experiment as follows:ethanol mass concentration of 65%,solid-liquid ratio of 1∶25(g∶mL),microwave irradiation power of 300 W,microwave irradiation time of 15 min(extracting for 5 times,once for 3 min).Under above conditions,the extraction rate of total flavones was 5.22%.The total flavones was characterized by UV and FTIR.The method was efficient,for it cost less time and energy with high extraction rate.
Keywords:persimmon leaves  total flavones  microwave extraction  orthogonal experiment  
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