| 二巯基丙磺酸钠的合成和表征 |
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| 引用本文： | 王秋伟. 二巯基丙磺酸钠的合成和表征[J]. 广东化工, 2010, 37(10): 33-34 |
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| 作者姓名： | 王秋伟 |
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| 作者单位： | 武汉工程大学化工与制药学院,湖北武汉430073; |
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| 摘 要： | 以丙烯磺酸钠为原料,经溴化、巯基化、成汞盐络合物、用硫化氢对络合物脱汞四个步骤合成二巯基丙磺酸钠,并对结构进行表征。
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| 关 键 词： | 二巯基丙磺酸钠 合成 结构表征 |
Synthesis and Characterization of Sodium Dimercaptosulfonate |
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| Wang Qiuwei. Synthesis and Characterization of Sodium Dimercaptosulfonate[J]. Guangdong Chemical Industry, 2010, 37(10): 33-34 |
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| Authors: | Wang Qiuwei |
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| Affiliation: | 1. School of Chemical Engineering and Pharmacy, Wuhan Institute of Technology, Wuhan 430073 ; 2. Key Laboratory of Novel Reactor and Green Chemical Technology of Hubei Province, Wuhan 430073, China) |
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| Abstract: | Sodium dimercaptosulfonate was synthesized from sodium allysufonate through four steps of bromination, sulfhydrylation, formation of mercury complex and decomposition of mercury salt with hydrogen sulfide. The structure of sodium dimercaptosulfonate was characterized by IR, ^1H NMR and ^13C and elemental analysis. |
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| Keywords: | sodiumdimercaptosulfonate synthesis structural characterization |
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