| 2,5-二[4-(4-溴苯氧基亚甲基)苯基]-1,3,4-噁二唑的合成与表征 |
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| 引用本文： | 邓继勇,黄赛金,廖云峰,党丽敏,刘碱.2,5-二[4-(4-溴苯氧基亚甲基)苯基]-1,3,4-噁二唑的合成与表征[J].化工新型材料,2009,37(12). |
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| 作者姓名： | 邓继勇 黄赛金 廖云峰 党丽敏 刘碱 |
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| 作者单位： | 湖南工程学院化学化工学院,湘潭,411104 |
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| 基金项目： | 湖南省自然科学基金资助项目，湖南省教育厅一般项目 |
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| 摘 要： | 以对甲基苯甲酸、水合肼为原料,通过关环、溴化、醚化合成了一种新型含噁二唑功能基有机聚合物电致发光材料单体2,5-二4-(4-溴苯氧基亚甲基)苯基]-1,3,4-噁二唑,其化学结构由红外光谱仪及核磁共振氢谱仪进行了表征,产品总收率22.64%.
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| 关 键 词： | 有机聚合物电致发光材料 噁二唑 单体 合成 |
Synthesis and charecterization of 2,5-bis[4-(4-bromophenoxymethylene) phenyl]-I, 3,4-oxadiazole |
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| Deng Jiyong,Huang Saijin,Liao Yunfeng,Dang Limin,Liu Jian.Synthesis and charecterization of 2,5-bis[4-(4-bromophenoxymethylene) phenyl]-I, 3,4-oxadiazole[J].New Chemical Materials,2009,37(12). |
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| Authors: | Deng Jiyong Huang Saijin Liao Yunfeng Dang Limin Liu Jian |
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| Abstract: | Using methylparaben and hydrazine hydrate as raw materials, by closing ring, bromination, etherifica-tion, a novel oxadiazole-functionalized monomer of organic polymer electroluminescent materials 2,5-bis4-(4-bromophe-noxymethylene)-1, 3,4-oxadiazole was synthesized, it's molecular structure was characterized by IR and ~1H NMR.The o-verall yield of the product was 22. 64%. |
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| Keywords: | organic polymer electrolumineseent material oxadiazole monomer synthesis |
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