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介质辅助微波消解用于火焰原子吸收测定沸石分子筛中Na
引用本文:张晓红,佘励勤.介质辅助微波消解用于火焰原子吸收测定沸石分子筛中Na[J].现代仪器,2007,13(2):68-70.
作者姓名:张晓红  佘励勤
作者单位:1. 北京北大先锋科技有限公司,北京100871
2. 北京大学化学与分子工程学院,北京100871
摘    要:利用介质辅助微波消解溶样,火焰原子吸收测量,准确测定分子筛中Na含量,加标回收率在92%~102%之间。介质辅助微波消解可使消解和赶酸一次进行,具有快速高效、酸消耗量小、安全清洁等优点。

关 键 词:介质辅助微波消解  沸石分子筛    火焰原子吸收

Application of dielectric assisted microwave digestion for determination of sodium in zeolite by FAAS
Zhang Xiaohong,She Liqin.Application of dielectric assisted microwave digestion for determination of sodium in zeolite by FAAS[J].Modern Instruments,2007,13(2):68-70.
Authors:Zhang Xiaohong  She Liqin
Affiliation:1. Beijing Peking University Pioneer Technology Co. Ltd. Beijing 100871 ;2. College of Chemistry and Molecular Engineering, Peking University Beijing 100871
Abstract:A method for determination of Na in zeolite by flame atomic absorption spectrometry(FAAS) after dielectric assisted microwave digestion for sample preparation was developed,with the recovery between 92%~102%.Assisted by dielectric,digestion,evaporation and cooling could be done in a single vessel by one step,so it was fast,clean and safe.
Keywords:Dielectric assisted microwave digestion Zeolite Na FAAS
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