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Reference Microgravity Measurements of Liquid Phase Solute Diffusivities in Tin- and Aluminum-Based Alloys
Authors:J. P. Garandet  G. Mathiak  V. Botton  P. Lehmann  A. Griesche
Affiliation:1. Commissariat à l'énergie Atomique, DRT/DTEN/SMP/LESA, CEA-Grenoble, 17 rue des Martyrs, F-38054, Grenoble Cedex 9, France
2. German Aerospace Center, DLR-RS, Linder Hoehe, D-51170, Cologne, Germany
3. EPM-Madylam, ENSHMG, BP 95, F-38402, St. Martin d'Hères Cedex, France
4. LMFA, INSA-Lyon, Batiment Joseph Jacquard, 20 avenue Albert Einstein, F-69621, Villeurbanne Cedex, France
5. Institute for Material Sciences and Technologies, TU Berlin, Hardenbergstr. 36, D-10623, Berlin, Germany
6. Hahn-Meitner-Institute (HMI) Berlin, Glienicker Str. 100, D-14109, Berlin, Germany
Abstract:This paper presents results of the measurement of solute diffusivities in the Al–Ni and Sn–Bi–In systems. These experiments were conducted in microgravity and may therefore be assigned as reference values. A dedicated facility, which can be used for processing of four identical samples in parallel, was developed for the experiments under consideration. In addition, a rather thorough analysis of possible error sources in shear cell type experiments is carried out. Comparison with work carried out using magnetic fields to control convective flows, and with previous indirect measurements results, is also provided. A coherent picture emerges from the overall agreement between various measurements, and the data from the current work can thus be considered as reference benchmarks for future experiments. Another conclusion of the present study is that the shear cell technique is well suited for the measurement of solute diffusivities.
Keywords:Al–  Ni system  composition measurement uncertainty  convection  error analysis  liquid-phase solute diffusion coefficients  low gravity  Sn–  In–  Bi system
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