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HPLC法测定从五倍子提取的单宁酸中焦性没食子酸的含量
引用本文:成春喜,耿芹. HPLC法测定从五倍子提取的单宁酸中焦性没食子酸的含量[J]. 化学与生物工程, 2007, 24(4): 73-74
作者姓名:成春喜  耿芹
作者单位:湖北省化学研究院,湖北,武汉,430074;湖北省化学研究院,湖北,武汉,430074
摘    要:在由五倍子提取的单宁酸中,通常存在着一定量的焦性没食子酸,采用乙腈、四氢呋喃和水在pH值为3的条件下利用Luna C18色谱柱可以很好地将焦性没食子酸与单宁酸中其它组分分离,并测定焦性没食子酸含量,该方法简单可行,已应用于工业生产.

关 键 词:单宁酸  焦性没食子酸  高效液相色谱
文章编号:1672-5425(2007)04-0073-02
修稿时间:2007-01-08

Determination of Pyrogallol Acid in Tannic Acid Extracted from Chinese Gallnut by High Performance Liquid Chromatography
CHENG Chun-xi,GENG Qin. Determination of Pyrogallol Acid in Tannic Acid Extracted from Chinese Gallnut by High Performance Liquid Chromatography[J]. Chemistry & Bioengineering, 2007, 24(4): 73-74
Authors:CHENG Chun-xi  GENG Qin
Affiliation:Hubei Research Institute of Chemistry, Wuhan 430074, China
Abstract:There are some pyrogallol acid in the tannic acid distilled from gallnut.The pyrogallol acid and other compositions can be well separated by HPLC on a Luna C_18 column with acetonitrile-tetrahydrofuran-water as mobile phase under the condition of pH=3.And the content of pyrogallol acid can be simply and successfully determined.This method has been applied in the industrial analysis.
Keywords:tannic acid  pyrogallol acid  HPLC
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