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Porous titanium (Ti) scaffolds by freezing TiH2/camphene slurries
Authors:Se-Won Yook  Hyoun-Ee Kim  Young-Hag Koh
Affiliation:a Department of Materials Science and Engineering, Seoul National University, Seoul, 151-742, Republic of Korea
b Department of Dental Laboratory Science and Engineering, Seoul, 136-703, Republic of Korea
c Department of Orthopaedic Surgery, Kang-Nam St. Mary's Hospital, The Catholic University of Korea, Seoul, 137-040, Republic of Korea
Abstract:Porous titanium (Ti) scaffolds with interconnected pores were fabricated by freezing titanium hydride (TiH2)/camphene slurries at 33 °C for 24 h, followed by freeze-drying and subsequent heat-treatment at 1300 °C for 2 h in vacuum. All of the fabricated samples revealed highly porous structures having large pores up to 100 μm in size surrounded by Ti metal walls without any secondary phases. When the initial TiH2 content was increased from 15 to 25 vol.%, the porosity was decreased from 63 to 49%, while the compressive strength was significantly improved from 81 to 253 MPa.
Keywords:Porous   Titanium (Ti)   Scaffold   Freeze casting   Bone tissue engineering
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