| 马来松香/SiO2杂化材料的研究 |
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| 引用本文： | 冯素好,王华林,江勤,汪文娟,黄君,余鹏.马来松香/SiO2杂化材料的研究[J].安徽化工,2010,36(1):44-46. |
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| 作者姓名： | 冯素好 王华林 江勤 汪文娟 黄君 余鹏 |
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| 作者单位： | 合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009;合肥工业大学化学工程学院,安徽合肥,230009 |
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| 摘 要： | 采用溶胶-凝胶法，以正硅酸乙酯（TEOS）为原料，制备硅溶胶；松香与马来酸酐熔融加成反应，生成马来松香；在对甲苯磺酸催化作用下，硅溶胶与马来松香发生酯化反应，生成马来松香／SiO2杂化材料。产物酸值较松香明显降低；FT-IR结果表明，其组份间以Si-O-C键键合；XRD结果表明，其为非晶态；DSC结果表明，其玻璃化转变温度㈣随着SiO2含量的增大而上升。
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| 关 键 词： | 硅溶胶 松香 马来松香 杂化材料 |
Research on Maleic Rosin/SiO2Hybrid Materials |
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| FENG Su-hao,WA NG Hua-lin,JIA NG-Qin,WA NG Wen-juan,HUANG Jun,YU Peng.Research on Maleic Rosin/SiO2Hybrid Materials[J].Anhui Chemical Industry,2010,36(1):44-46. |
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| Authors: | FENG Su-hao WA NG Hua-lin JIA NG-Qin WA NG Wen-juan HUANG Jun YU Peng |
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| Affiliation: | School ofChemical Technology;Hefei UniversityofTechnology;Hefei 230009;China |
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| Abstract: | Silica sol were prepared by sol-gel method,using tetraethyl orthosilicate(TEOS)as raw materials. Maleic rosin were prepared by melt rosin and maleic anhydride addition reaction. In p-toluenesulfonic acid catalyst,maleic rosin/SiO2 hybrid materials were prepared,occuring the silica sol with maleic rosin esterification reaction. Acid of hybrid materials were significantly lower than the rosin. FT-IR patterns present that their phrases were connected with Si-O-C bonds. XRD patterns present that they were amorp... |
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| Keywords: | silica sol rosin maleic rosin hybrid material |
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