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苦荞糊和苦荞茶挥发性香气成分分析
引用本文:余丽,王灼琛,程江华,谢宁宁,黄晶晶.苦荞糊和苦荞茶挥发性香气成分分析[J].中国酿造,2014(10):67-71.
作者姓名:余丽  王灼琛  程江华  谢宁宁  黄晶晶
作者单位:安徽省农业科学院农产品加工研究所;
基金项目:2014年学科建设面上项目(14A1231);2014年新建科技创新团队(14C1207);2013年公益性行业(农业)科研专项项目(201303069)
摘    要:采用固相微萃取法(SPME)对苦荞茶和苦荞糊中的挥发性香气成分进行提取,并经气相色谱-质谱联用(GC-MS)技术定性分析。从苦荞茶和苦荞糊中分别检测出30种和41种挥发性香气成分,相同成分有15种,其中含量较高的是烃类、醛类和杂环类,三者在苦荞茶和苦荞糊中含量分别为24.56%、35.04%、18.42%和46.97%、21.22%、7.22%。研究表明,顶空固相微萃取具有快速简便、不使用溶剂和样品检测非破坏性等优点,结合气-质联用技术可以很好的分析苦荞产品中挥发性物质,并说明不同加工工艺制得的苦荞产品其挥发性物质存在一定差异。

关 键 词:苦荞茶  苦荞糊  挥发性成分  固相微萃取  气相色谱-质谱法

Analysis of volatile aroma compounds in tartary buckwheat paste and tartary buckwheat tea
YU Li,WANG Zhuochen,CHENG Jianghua,XIE Ningning,HUANG Jingjing.Analysis of volatile aroma compounds in tartary buckwheat paste and tartary buckwheat tea[J].China Brewing,2014(10):67-71.
Authors:YU Li  WANG Zhuochen  CHENG Jianghua  XIE Ningning  HUANG Jingjing
Affiliation:(Institute of Agro-Products Processing Science and Technology, Anhui Academy of Agricultural Sciences, Hefei 230031, China)
Abstract:The volatile aroma components in tartary buckwheat tea and tartary buckwheat paste were extracted by solid phase microextraction(SPME)technique and determined by GC-MS. Thirty volatile compounds were isolated and identified from tartary buckwheat tea, and forty-one compounds from tartary buckwheat paste, in which fifteen compounds were common to both. The contents of hydrocarbons, aldehydes and heterocyclic compounds were 24.56%, 35.04%, 18.42% in tartary buckwheat tea and 46.97%, 21.22%, 7.22% in tartary buckwheat paste, respectively. The study showed that SPME method provided a good result combing with GC-MS in detecting volatile compounds of tartary buckwheat products with advantages of rapid,simple, and non-destructive, and there were some differences in volatile substances of buckwheat products with different processing technology.
Keywords:tartary buckwheat tea  tartary buckwheat paste  volatile components  solid phase microextraction  GC-MS
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