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气质联用法测定鞋类橡胶材料中的N-亚硝基胺含量
引用本文:童玉贵,林伟,林中,方光伟,程群.气质联用法测定鞋类橡胶材料中的N-亚硝基胺含量[J].皮革科学与工程,2011,21(5).
作者姓名:童玉贵  林伟  林中  方光伟  程群
作者单位:莆田出入境检验检疫局,福建莆田,351100
摘    要:鞋类产品的橡胶材料中的N-亚硝基胺经甲醇提取,提取液浓缩后经C18小柱净化,气质联用法测定样液中的N-亚硝基胺含量。方法灵敏度高,回收率及精密度均较满意,可应用于鞋类橡胶材料中N-亚硝基胺的检测。

关 键 词:N-亚硝基胺  气质联用法  鞋类产品  橡胶材料  

Determination of N-nitrosamines in Rubber Materials of Shoes by GC-MS
TONG Yu-gui,LIN Wei,LIN Zhong,FANG Guang-wei,CHENG Qun.Determination of N-nitrosamines in Rubber Materials of Shoes by GC-MS[J].Leather Science and Engineering,2011,21(5).
Authors:TONG Yu-gui  LIN Wei  LIN Zhong  FANG Guang-wei  CHENG Qun
Affiliation:TONG Yu-gui,LIN Wei,LIN Zhong,FANG Guang-wei,CHENG Qun(Putian Entry-Exit Inspection and Quarantine Bureau,Putian 351100,China)
Abstract:The N-nitrosamines in rubber materials of shoes are extracted by alcohol,and then the sample solution is concentrated and then cleaned by C18 column.GC-MS was used to detect the content.The method has good sensitivity,high recovery,and good precise,and can be used to detect the N-nitrosamines in rubber materials of shoes.
Keywords:GC-MS  N-nitrosamines  shoe  rubber material  
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