| Trans-3-甲基-4-溴-2-丁烯基苄基醚的合成研究 |
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| 引用本文： | 黄建平,张招贵,陈芬儿. Trans-3-甲基-4-溴-2-丁烯基苄基醚的合成研究[J]. 江西化工, 2006, 0(2): 10-11 |
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| 作者姓名： | 黄建平 张招贵 陈芬儿 |
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| 作者单位： | 南昌大学,化学系,江西,南昌,330047;复旦大学,化学系,上海,200031 |
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| 摘 要： | 目的：合成Trans-3-甲基-4-溴-2-丁烯基苄基醚。方法：以3-甲基-2-丁烯基-1-醇为起始原料，经三步反应制得目标化合物。结果与结论：各步中间体结构经核磁共振谱、质谱确证，总收率为61．6％,探索出一条新的合成路线。
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| 关 键 词： | 3-甲基-2-丁烯基苄基醚 反式4-溴-3-甲基-2-丁烯基苄基醚 氧化 合成 |
Study on Synthesis of (trans-4-bromo-3-methyl-2-butenyl) oxymethyl benzene |
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| HUANG Jian-ping,ZHANG Zhao-gui,CHEN Fen-er. Study on Synthesis of (trans-4-bromo-3-methyl-2-butenyl) oxymethyl benzene[J]. Jiangxi Chemical Industry, 2006, 0(2): 10-11 |
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| Authors: | HUANG Jian-ping ZHANG Zhao-gui CHEN Fen-er |
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| Abstract: | Objective: To prepare(trans-4-bromo-3-methyl-2-butenyl)oxymethyl benzene.Methods:The target compound was synthesized by three steps with(3-methyl-2-butenyl)oxymethyl benzene.Results and Conclusions: A new sysnthesis round was explored.the desired product was obtained in over all yield of 61.6 %and its structure was confirmed by ~1?H-NMR and MS. |
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| Keywords: | (3-methyl-2-butenyl)oxymethyl benzene(trans-4-bromo-3-methyl-2-butenyl) Oxymethyl benzene Oxidation synthesis. |
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