| 超临界CO2萃取烟草中茄尼醇的工艺条件优化 |
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| 引用本文： | 高文义,王姣,秦思,黄德春,王志祥. 超临界CO2萃取烟草中茄尼醇的工艺条件优化[J]. 化工时刊, 2010, 24(10): 29-31. DOI: 10.3969/j.issn.1002-154X.2010.10.008 |
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| 作者姓名： | 高文义 王姣 秦思 黄德春 王志祥 |
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| 作者单位： | 浙江国邦药业有限公司,浙江,上虞,312369;中国药科大学,药学院,江苏,南京,210009;中国药科大学,生命科学与技术学院,江苏,南京,210009 |
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| 摘 要： | 采用超临界CO2萃取烟草中的茄尼醇,以茄尼醇的质量收率为考察指标,以萃取温度、萃取压力、萃取时间、夹带剂浓度、夹带剂流量为考察因素进行正交实验,优选最佳的萃取工艺条件。最佳的萃取工艺条件为:萃取温度40℃,萃取压力35MPa,萃取时间2h,夹带剂无水乙醇,夹带剂流量0.3mL·min-1。在此实验条件下,茄尼醇的平均质量收率为0.8288%。
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| 关 键 词： | 超临界CO2 萃取 烟草 茄尼醇 优化 |
Optimization of the Technology of Supercritical CO2 Extraction Solanesol from Tobacco Leaves |
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| Gao Wenyi,Wang Jiao,Qin Si,Huang Dechun,Wang Zhixiang. Optimization of the Technology of Supercritical CO2 Extraction Solanesol from Tobacco Leaves[J]. Chemical Industry Times, 2010, 24(10): 29-31. DOI: 10.3969/j.issn.1002-154X.2010.10.008 |
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| Authors: | Gao Wenyi Wang Jiao Qin Si Huang Dechun Wang Zhixiang |
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| Affiliation: | Gao Wenyi Wang Jiao Qin Si Huang Dechun Wang Zhixiang(1. Zhejiang Guobang Pharmaceutical Co.,Ltd,Zhejiang Shangyu 312369; 2. School of Pharmacy,China Pharmaceutical University,Jiangsu Nanjing 210009; 3. School of Life Science andTechnology,China Pharmaceutical University,Jiangsu Nanjing 210009) |
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| Abstract: | Supercritical CO2 fluid was used to extract Solanesol from Tobacco Leaves. The quality yield of Solanesol was used as the evaluation index and extraction temperature、extraction pressure、the flow-rate of CO2、the concentration of entrainer and the flow rate of entrainer as affecting factors,the optimal extraction process was determined by orthogonal experiments. The optimum extraction process was set as follows：extraction temperature at 40 ℃,extraction pressure under 35 MPa,extraction time 2 h,absolute ethyl alcohol as the entrainer,the flow rate of entrainer was 0. 3 mL-1·min-1,in this experimental condition,the average quality yield of Solanesol was 0.8288%. |
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| Keywords: | supercritical CO2 extraction tobacco leaves sloanesol optimization |
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