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The pressure drop experiment to determine slug lengths in multiphase monoliths
Authors:Michiel T. Kreutzer   Menno G. van der Eijnden   Freek Kapteijn   Jacob A. Moulijn  Johan J. Heiszwolf
Affiliation:

aReactor and Catalysis Engineering, DelftChemTech, Faculty of Applied Sciences, Delft University of Technology, Julianalaan 136, 2628 BL Delft, The Netherlands

bAlbemarle Catalyst Company BV, Nieuwendammerkade 1-3, P.O. Box 37650, 1030 BE Amsterdam, The Netherlands

Abstract:The length of the liquid slugs, that separate the elongated bubbles in Taylor flow, is an important parameter for mass transfer, flow stability and pressure drop in capillary microchannels. In this work, pressure drop measurements are used to determine the length of slug in Taylor flow in downflow monoliths. The method is sensitive if the slugs are relatively short, less than 10 times the channel diameter. The pressure drop measurements are a cheap and fast alternative to tomographic or electric methods. Experiments using different distributors indicate that the slug length varies significantly with changes in the hydrodynamics in the feed section of the monoliths. Slug length correlations that are based on parameters inside the channels can therefore not safely be used for a different setup. As a result, the slug length should be measured in each experimental setup, which makes a inexpensive and robust method to do so very welcome.
Keywords:Pressure drop   Taylor flow   Monoliths   Multiphase reactors   Fluid mechanics
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