| 四氯化锡催化合成β-萘甲醚 |
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| 引用本文： | 姚碧霞,翁文,沈淑君,陈慧敏.四氯化锡催化合成β-萘甲醚[J].应用化工,2004,33(3):26-27. |
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| 作者姓名： | 姚碧霞 翁文 沈淑君 陈慧敏 |
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| 作者单位： | 漳州师范学院,化学系,福建,漳州,363000 |
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| 基金项目： | 福建省高校重点科技项目(JA99210)，福建省科技厅项目(K02092) |
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| 摘 要： | 四氯化锡催化下,β 萘酚与无水甲醇反应合成β 萘甲醚,考察了甲醇用量、催化剂用量、反应时间等对产率的影响。当β 萘酚取1.8g,甲醇1.5mL,SnCl4·5H2O取0.33g时,80℃反应10h,β 萘甲醚产率可达75.3%。
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| 关 键 词： | 四氯化锡 β-萘甲醚 催化合成 |
| 文章编号： | 1671-3206(2004)03-0026-02 |
| 修稿时间： | 2004年1月9日 |
Catalytic synthesis of β-naphthol methyl ether with tin tetrachloride |
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| YAO Bi-xia,WENG Wen,SHEN Shu-jun,CHEN Hui-min.Catalytic synthesis of β-naphthol methyl ether with tin tetrachloride[J].Applied chemical industry,2004,33(3):26-27. |
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| Authors: | YAO Bi-xia WENG Wen SHEN Shu-jun CHEN Hui-min |
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| Abstract: | β-naphthol methyl ether was catalytically synthesized by tin tetrachloride. The effects of the dosage of methanol and SnCl_4·5H_2O, reaction time on the yield of β-naphthol methyl ether were studied. When the amount of β-naphthol was 1.8 g, methanol was 1.5 mL, SnCl_4·5H_2O was 0.33 g, 80℃ reacted for 10 h,the yield of β-naphthol methyl ether may up to 75.3%. |
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| Keywords: | tin tetrachloride β-naphthol methyl ether catalytic synthesis |
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