| 对位取代查尔酮衍生物的合成 |
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| 引用本文： | 董秋静,罗春华.对位取代查尔酮衍生物的合成[J].精细化工中间体,2007,37(5):31-33,39. |
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| 作者姓名： | 董秋静 罗春华 |
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| 作者单位： | 1. 安徽建筑工业学院,材料与化学工程学院,安徽,合肥,230022
2. 中国科学院,成都有机化学研究所,四川,成都,610041 |
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| 基金项目： | 安徽建筑工业学院校科研和教改项目 |
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| 摘 要： | 以苯甲醛和苯乙酮衍生物为原料,在氢氧化钠乙醇水溶液中,室温制备了一系列的查尔酮衍生物,收率在60%～90%之间。并通过熔点、凝胶渗透色谱、紫外光谱、红外光谱和核磁共振氢谱对其结构进行了表征。
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| 关 键 词： | 对羟基查尔酮 4-羟基-4'-溴查尔酮 4 4'-二溴查尔酮 |
| 文章编号： | 1009-9212（2007）05-0031-03 |
| 修稿时间： | 2007-05-09 |
Synthesis of p-Substituted Chalcone Derivatives |
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| DONG Qiu-jing,LUO Chun-hua.Synthesis of p-Substituted Chalcone Derivatives[J].Fine Chemical Intermediates,2007,37(5):31-33,39. |
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| Authors: | DONG Qiu-jing LUO Chun-hua |
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| Affiliation: | 1. Department of Material and Chemistry Engineering, Anhui Institute of Architecture and Industry, Hefei 230022, China; 2. Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu 610041, China |
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| Abstract: | A series of chalcone derivatives with yield from 60% to 90% were synthesized from benzaldehyde and acetophenone derivatives in NaOH/ethanol/H2O solution at room temperature. The structures were characterized by melting point,GPC,FT-IR,1H NMR. |
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| Keywords: | p-hydroxychalcones 4-hydroxy-4'-bromo-chalcone 4 4'-dibromochalcone |
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