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Investigation into microstructure of carbon nanotube multi-yarn
Affiliation:1. Air Force Institute of Technology, Department of Aeronautics and Astronautics, 2950 Hobson Way, Wright-Patterson AFB, OH 45433-7765, United States;2. Wichita State University, Department of Mechanical Engineering, 1845 Fairmount, Wichita, KS 67260-0133, United States;1. Architecture and Civil Engineering Institute, Guangdong University of Petrochemical Technology, Maoming 525000, China;2. Key Laboratory of Flexible Electronics (KLOFE) & Institute of Advanced Materials (IAM), Jiangsu National Synergistic Innovation Center for Advanced Materials (SICAM), Nanjing Tech University (NanjingTech), Nanjing 211816, China;3. School of Computer and Electronic Information, Guangdong University of Petrochemical Technology, Maoming 525000, China;1. U.S. Army Research Laboratory, Aberdeen Proving Ground, MD, 21005-5069, USA;2. Department of Mechanical Engineering, University of Maryland, College Park, MD, 20742, USA;3. Department of Aeronautics and Astronautics, Massachusetts Institute of Technology, Cambridge, MA, 02139, USA;1. Shanghai Key Laboratory of Lightweight Composite, Donghua University, Shanghai 201620, PR China;2. College of Textiles, Donghua University, Shanghai 201620, PR China;3. College of Fashion Technology, Shanghai University of Engineering Science, Shanghai 201620, PR China;1. IMDEA Materials Institute, 28906, Getafe, Madrid, Spain;2. Universidad Autónoma de Madrid, 28049, Madrid, Spain;3. Institute of Advanced Composite Materials, Korea Institute of Science and Technology (KIST), 55324, Jeonbuk, Republic of Korea;4. IMDEA Nanociencia, Calle Faraday 9, Cantoblanco, 28049, Madrid, Spain;5. Polytechnic University of Madrid, E. T. S. de Ingenieros de Caminos, 28040, Madrid, Spain
Abstract:Structural analysis at the nano and micro scale was performed on a carbon nanotube (CNT) multi-yarn. The yarns were made by a process of drawing CNTs into a ribbon and twisting the ribbon into a yarn. Scanning electron microscopy (SEM) was used to view the exterior of the yarn. Polarized microscopy was used to examine details of the 1-yarn, and it also identified ribbon–ribbon boundaries. Further examination of interior structure was done by NanoCT scans which showed that folding of the ribbons had occurred causing complicated structures. The interior folding was found by milling into the yarn with a focus ion beam gun (FIB) and imaging with SEM. These different methods thus provided various microstructural details (structure, ribbon–ribbon boundary, folding and void fraction) of CNT multi-yarn which could be used to compare with other yarns fabricated with different procedures/sources as well to provide parameters for analytical tools. Further, these microstructural details can be related to macro mechanical and physical properties.
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