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Cobalt oxide nanopowder synthesis using cellulose assisted combustion technique
Affiliation:1. Faculty of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, PR China;2. College of Materials Science and Engineering, Wuhan Textile University, Wuhan 430073, PR China;3. Henan Province Industrial Technology Research Institute of Resources and Materials, Zhengzhou University, Zhengzhou 450001, PR China;4. Department of Chemistry and Physics, Fayetteville State University, Fayetteville, NC 28301, USA
Abstract:Cobalt oxides nanopowders were prepared using novel cellulose assisted combustion synthesis and solution combustion synthesis techniques. The synthesis conditions were optimized to produce high surface area cobalt oxide nanopowders. Effect of precursors ratio on product properties (such as crystalline structure, nanoparticle size, surface area etc.) were studied and compared for the two methods. Thermodynamic calculations along with TGA/DTA studies were used to understand the synthesis mechanism leading to cobalt oxide formation. The synthesized nanopowders were characterized using various materials characterization techniques such as XRD, SEM and TEM.
Keywords:Cellulose assisted combustion synthesis  Solution combustion synthesis  Impregnated layer combustion synthesis  Cobalt oxide nanopowder
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