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Aflatoxin M1 survey on randomly collected milk powder commercialized in Argentina and Brazil
Affiliation:1. Departamento de Industrias y Química Orgánica, Facultad de Ciencias Exactas y Naturales (FCEN), Universidad de Buenos Aires (UBA), Intendente Güiraldes 2160, 1428 Ciudad Universitaria, Buenos Aires, Argentina;2. Departamento de Industrias, Facultad de Ciencias Exactas y Naturales (FCEN), Universidad de Buenos Aires (UBA), Intendente Güiraldes 2160, Ciudad Universitaria, Buenos Aires, Argentina;3. Programa de Pós-Graduação em Ciências e Tecnologia de Alimentos, Centro de Ciências Agrárias, Universidade Federal de Santa Catarina (UFSC), Rodovia Admar Gonzaga, 1346, Itacorubí, Florianópolis, CEP 88034-001, SC, Brazil;4. Departamento de Ciências e Tecnologia de Alimentos, Centro de Ciências Agrárias, Universidade Federal de Santa Catarina (UFSC), Rodovia Admar Gonzaga, 1346, Itacorubí, Florianópolis, CEP 88034-001, SC, Brazil;5. Comisión de Investigaciones Científicas de la Provincia de Buenos Aires (CIC), Calle 526 entre 10 y 11, La Plata, Provincia de Buenos Aires, Argentina;6. Fundación de Investigaciones Científicas Teresa Benedicta de la Cruz, Dorronzoro 141, 6700 Luján, Buenos Aires, Argentina;1. University of Prishtina, Faculty of Agriculture and Veterinary, Prishtina, Kosovo, Serbia;2. Food and Veterinary Agency, Prishtina, Kosovo, Serbia;3. National Institute of Public Health of Kosovo, Serbia;1. Department of Nutritional Physiology and Feeding, Agricultural University of Athens, Iera Odos 75, GR-11855 Athens, Greece;2. Pesticide Residues Laboratory, Department of Pesticides Control and Phytopharmacy, Benaki Phytopathological Institute, GR-145 61 Kifissia, Greece;3. Laboratory of General Chemistry, Science Department, Agricultural University of Athens, Iera Odos 75, GR-118 55 Athens, Greece;1. Laboratory for Residue Control, Department of Veterinary Public Health, Croatian Veterinary Institute, Savska cesta 143, HR-10000 Zagreb, Croatia;2. General Department, Croatian Veterinary Institute, Savska cesta 143, HR-10000 Zagreb, Croatia;1. Institute of Food Science & Nutrition, Bahauddin Zakariya University, Multan, Pakistan;2. Department of Food Science, University of Massachusetts Amherst, Amherst, USA;3. Department of Food Science and Technology, College of Life Sciences, Sejong University, Gunja-dong 98, Gwangin-gu, Seoul 143-747, Republic of Korea;4. Institute for Global Food Security, Queens University Belfast, UK;5. Department of Food Engineering, School of Animal Science and Food Engineering, University of São Paulo, Brazil;1. Department of Food Hygiene and Quality Control, Faculty of Veterinary Medicine, Razi University, Kermanshah, Iran;2. Department of Clinical Sciences, Faculty of Veterinary Medicine, Razi University, Kermanshah, Iran;3. Department of Food Hygiene and Quality Control, Faculty of Veterinary Medicine, University of Tehran, Tehran, Iran
Abstract:Aflatoxin M1 (AFM1), the main monohydroxylated of aflatoxin B1 (AFB1) formed in liver and excreted in the milk, has toxicological proprieties comparable to those of AFB1, albeit a lower carcinogenic potency. The presence of AFM1 was investigated in 30 samples of powdered milk purchased in Argentina and Brazil. The samples were analyzed using an immunoaffinity column for cleanup and HPLC-FLD for determining AFM1. The quantification limit was 0.1 μg/kg. AFM1 was found in all the samples at levels ranging from 0.1 to 0.92 μg kg−1 with average concentration of 0.39 μg kg−1.
Keywords:Powder milk  HPLC
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