| 丙烯酸正丁酯的新型催化合成 |
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| 引用本文： | 唐薰,夏涛,张长利,焦佩玉.丙烯酸正丁酯的新型催化合成[J].精细化工中间体,2002,32(3):23-24. |
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| 作者姓名： | 唐薰 夏涛 张长利 焦佩玉 |
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| 作者单位： | 1. 湖南大学化学化工学院,湖南,长沙,410082
2. 长沙贞观科技开发有限公司,湖南,长沙,410007 |
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| 摘 要： | 丙烯酸与正丁醇在金属盐类固体催化剂的作用下合成丙烯酸正丁酯 ,收率可达到98 1%,采用减压蒸馏能得到纯度为 99%以上的产品。探讨了各个因素对产品收率的影响 ,给出了最佳反应条件。
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| 关 键 词： | 丙烯酸 固体催化剂 丙烯酸正丁酯 催化酯化 |
| 文章编号： | 1009-9212(2002)03-0023-02 |
| 修稿时间： | 2001年10月18 |
Synthesis of N-butyl Acrylate by Novel Catalyst |
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| Tang Xun ,Xia Tao ,Zhang Chang-li ,Jiao Pei-yu.Synthesis of N-butyl Acrylate by Novel Catalyst[J].Fine Chemical Intermediates,2002,32(3):23-24. |
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| Authors: | Tang Xun Xia Tao Zhang Chang-li Jiao Pei-yu |
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| Affiliation: | Tang Xun 1,Xia Tao 1,Zhang Chang-li 2,Jiao Pei-yu 2 |
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| Abstract: | The synthesis of n-butyl acrylate from acrylic acid and n-butyl alcohol in the presence of a novel solid catalyst was studied .The yield of n-butyl drylate was 98.1%.The purity of product may exceed 99% by reducetng pressure distillation. The factors effecting the yield of the product and the optimum reaction conditions were offered. |
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| Keywords: | acrylic acid solid catalyst n-butyl acrylate catalytic esterification |
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