| Study on Enhancement in Gibbsite Precipitation of Bayer Process under 33 kHz Ultrasound |
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| 作者姓名： | JihuaZHAO QiyuanCHEN |
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| 作者单位： | CollegeofChemistryandChemicalEngineering,CentralSouthUniversity,Changsha410083,China |
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| 摘 要： | The enhancement of gibbsite precipitation in Bayer process by 33 kHz ultrasound has been studied. From orthomethod experiment, the optimized operating parameters of treatment under 33 kHz ultrasonic cleaner have obtained.Compared with crystallization of Al(OH)3 without treatment of ultrasound, the precipitation time is reduced by 15 h when the precipitation ratio is 45%. From the results of grain size distribution and SEM photographs of gibbsite, it is found that secondary nucleation and agglomeration could be enhanced under 33 kHz ultrasound. The products are same from comparison of X-ray powder diffraction, but the Raman spectrum of sodium aluminate solution under 33 kHz ultrasound is different from that without ultrasound.
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| 关 键 词： | 水铝矿 超声波 Al（OH）3 X-射线衍射 拉曼光谱 |
Study on Enhancement in Gibbsite Precipitation of Bayer Process under 33 kHz Ultrasound |
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| JihuaZHAO QiyuanCHEN.Study on Enhancement in Gibbsite Precipitation of Bayer Process under 33 kHz Ultrasound[J].Journal of Materials Science & Technology,2003,19(6):607-610. |
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| Authors: | Jihua ZHAO Qiyuan CHEN |
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| Affiliation: | College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China;College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 730000, China |
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| Abstract: | The enhancement of gibbsite precipitation in Bayer process by 33 kHz ultrasound has been studied. From orthome-thod experiment, the optimized operating parameters of treatment under 33 kHz ultrasonic cleaner have obtained. Compared with crystallization of AI(OH)3 without treatment of ultrasound, the precipitation time is reduced by 15 h when the precipitation ratio is 45%. From the results of grain size distribution and SEM photographs of gibbsite, it is found that secondary nucleation and agglomeration could be enhanced under 33 kHz ultrasound. The products are same from comparison of X-ray powder diffraction, but the Raman spectrum of sodium aluminate solution under 33 kHz ultrasound is different from that without ultrasound. |
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| Keywords: | Ultrasound Aluminium trihydroxide Precipitation |
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