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Comparative evaluation of microwave‐assisted extraction and preheated solvent extraction of bioactive compounds from a plant material: a case study with cabbages
Authors:Watsapol Sookjitsumran  Sakamon Devahastin  Arun S Mujumdar  Naphaporn Chiewchan
Affiliation:1. Advanced Food Processing Research Laboratory, Department of Food Engineering, Faculty of Engineering, King Mongkut's University of Technology Thonburi, Tungkru, Bangkok, Thailand;2. PTT Group Frontier Research Center, PTT Public Company Limited, Bangkok, Thailand
Abstract:Preheated solvent extraction (PSE) was evaluated via the analysis of the extraction kinetics, microstructure of extracted samples and energy consumption as alternative to microwave‐assisted extraction (MAE). Cabbage outer leaves and ethanol were used as test material and extraction solvent, respectively. MAE was first optimised in terms of glucosinolates and phenolics yields; total antioxidant activity of the extracts was also assessed. MAE at a specific absorbed power of 0.37 W g?1 for 9 min was selected as optimum condition to extract glucosinolates and phenolics, while PSE was optimised at 6 min of the extraction. The highest normalised total glucosinolates and phenolic contents as well as antioxidant activities of the extracts obtained via MAE were not significantly different from those obtained via PSE. Confocal laser scanning microscopy revealed no significant differences in cabbage cell damages rendered by MAE and PSE. PSE nevertheless exhibited slightly higher specific energy consumption than MAE.
Keywords:Bioactive compounds  energy consumption  fractal analysis  microstructure  Soxhlet extraction  temperature evolution
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