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MnFe2O4纳米晶体的制备及表征
引用本文:王秀宇,杨桂琴,严乐美,孟建华,孙艺环.MnFe2O4纳米晶体的制备及表征[J].化学工业与工程,2004,21(2):84-86,90.
作者姓名:王秀宇  杨桂琴  严乐美  孟建华  孙艺环
作者单位:天津大学理学院,天津,300072;天津大学理学院,天津,300072;天津大学理学院,天津,300072;天津大学理学院,天津,300072;天津大学理学院,天津,300072
摘    要:本文分别采用低温共沉淀法、高温法和水热法制备MnFe2O4的纳米晶体。利用XRD、TEM和VSM对试样进行了表征。重点研究了低温共沉淀法的制备方法。通过对三种方法的对比分析,试验结果表明低温共沉淀法适宜制备小粒径的MnFe2O4。

关 键 词:低温共沉淀法  尖晶石  纳米晶体MnFe2O4
文章编号:1004-9533(2004)02-0084-03

The Synthesis of MnFe2O4 Nanocrystals and Their Characterization
WANG Xiu-yu,YANG Gui-qin,YAN Le-mei,MENG Jian-hua,SUN Yi-huan.The Synthesis of MnFe2O4 Nanocrystals and Their Characterization[J].Chemical Industry and Engineering,2004,21(2):84-86,90.
Authors:WANG Xiu-yu  YANG Gui-qin  YAN Le-mei  MENG Jian-hua  SUN Yi-huan
Abstract:MnFe_2O_4 nanocrystals were prepared by low-temperature coprecipitation method,high temperature method and hydrothermal method respectively.And the samples obtained by the three methods were characterized by XRD,TEM and VSM.The preparation for MnFe_2O_4 nanocrystals using precursor with low-temperature coprecipitation method was studied in detail.Comparison and analysis of the three methods indicated that low-temperature coprecipitation method was optimal in the preparation of pure samples with small size.
Keywords:low-temperature coprecipitation method  spinel  MnFe_2O_4 nanocrystals  
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