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Pyrolytic Synthesis of Carbon Nanotubes from Sucrose on a Mesoporous Silicate
Authors:Tarek Abdel-Fattah  Emilie J Siochi  Roy E Crooks
Affiliation:  a Department of Biology, Chemistry and Environmental Science Christopher Newport University, Newport News, Virginia, USA b Advanced Materials and Processing Branch, NASA Langley Research Center, Hampton, Virginia, USA c National Institute of Aerospace Hampton, Virginia, USA
Abstract:Multi-wall carbon nanotubes were synthesized from sucrose by a pyrolytic technique using mesopourous MCM-41 silicate templates without transition metal catalysts. The nanotubes were examined in the carbon/silicate composite and after dissolution of the silicate. High-resolution transmission electron microscopy study of the multi-wall nanotubes showed them to be 15 nm in diameter, 200 nm in length and close-ended. There was variation in crystallinity with some nanotubes showing disordered wall structures.
Keywords:pyrolytic synthesis  multi-wall carbon nanotubes  mesopourous  templates
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