Synthesis of Sn2P2S6 |
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Authors: | I. N. Rybina T. G. Lupeiko S. N. Svirskaya A. A. Nesterov |
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Affiliation: | 1.Southern Federal University,Rostov-on-Don,Russia |
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Abstract: | A process that presents no explosion hazard is proposed for the preparation of tin(II) hexathiohypodiphosphate(IV) in a limited amount of air. The reaction of tin(II) sulfide with a mixture of phosphorus sulfides with the overall composition “P4S8” is studied, and the influence of synthesis temperature and duration on the completion of the reaction is analyzed. |
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